Overview

This complete laboratory reference manual explains the principles behind solid phase extraction (SPE) and provides readily reproducible protocols for solving extraction problems in forensic and clinical chemistry. Numerous actual chromatograms, based on original research and diverse applications, demonstrate the technique and the results that can be achieved. Extensive appendices allow fast access to frequently needed information on reagents, the preparation of solutions and buffers, milliequivalent and millimode calculations, buffers and pKa for SPE, and a complete RapidTrace® technical manual. Each proven protocol is described in step-by-step detail and contains an introduction outlining the principle behind the technique, lists of equipment and reagents, and tips on troubleshooting and on avoiding known pitfalls.

Full Product Details

Author:   Michael J. Telepchak
Publisher:   Humana Press Inc.
Imprint:   Humana Press Inc.
Edition:   Softcover reprint of the original 1st ed. 2004
Dimensions:   Width: 17.80cm , Height: 2.00cm , Length: 25.40cm
Weight:   0.728kg
ISBN:  

9781617371141

ISBN 10:   1617371149
Pages:   370
Publication Date:   19 November 2010
Audience:   Professional and scholarly ,  Professional & Vocational
Replaced By:   9781603273589
Format:   Paperback
Publisher's Status:   Active
Availability:   In Print  
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Table of Contents

1: Introduction to Solid Phase Extraction.- 2: Silica-Based Solid Phase Extraction.- 3: The Chemistry of Bonded Silicas.- 4: Bonded Phase Sorbent Synthesis.- 5: Strategies for the Use of Solid Phase Extraction.- 6: Optimizing Solid Phase Extraction Methods.- 7: Separation of Analytes from Their Matrices.- 8: Solid Phase Extraction Troubleshooting.- 9: Drug Methods for the Toxicology Lab.- 10: Selected Solid Phase Extraction Applications in Drug Analysis.- 11: General Methods for Drug Isolation.- 12: Chemical Derivatization.- Appendix A: Glossary.- Appendix B: Reagents.- Appendix C: Preparation of Solutions and Buffers.- Appendix D: Milliequivalent and Millimole Calculations.- Appendix E: Selected Solvent Polarity and Property Scale.- Appendix F: Buffers for Solid Phase Extraction.- Appendix I: Further Reading.

Reviews

... a recommended addition to the laboratory shelf, as a training aid and also as a a convenient source of SPE methodolgical and analytical data. -ASCLD This book is detailed, well organized, and is an excellent laboratory reference manual for the application of SPE to forensic or clinical analyses. - Canadian Society of Forensic Science Journal

... a recommended addition to the laboratory shelf, as a training aid and also as a a convenient source of SPE methodolgical and analytical data. -ASCLD This book is detailed, well organized, and is an excellent laboratory reference manual for the application of SPE to forensic or clinical analyses. - Canadian Society of Forensic Science Journal

"""... a recommended addition to the laboratory shelf, as a training aid and also as a a convenient source of SPE methodolgical and analytical data."" -ASCLD ""This book is detailed, well organized, and is an excellent laboratory reference manual for the application of SPE to forensic or clinical analyses."" - Canadian Society of Forensic Science Journal"

... a recommended addition to the laboratory shelf, as a training aid and also as a a convenient source of SPE methodolgical and analytical data. -ASCLD This book is detailed, well organized, and is an excellent laboratory reference manual for the application of SPE to forensic or clinical analyses. - Canadian Society of Forensic Science Journal

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